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Modern Instrumental Methods of Analysis

IISc Bangalore Course , Prof. J.R. Mudakavi       Subscribe to feed

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Lecture 1: Mod-01 Lec-01 Introduction to the Modern Instrumental Methods of Analysis

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Lecture Details :

Modern Instrumental Methods of Analysis by Dr. J.R. Mudakavi ,Department of Chemical Engineering, IISC Bangalore. For more details on NPTEL visit http://nptel.iitm.ac.in

Course Description :

This course is designed to familiarize the students with various instrumental methods of chemical analysis that scientists and engineers come across during their course work and research undertakings.
The participants are introduced to the principles of chemical analysis, matrix effects, detailed instrumentation, operation and interpretation of data, error analysis and statistical methods of data handling.
At the end of the course the student would be able to handle the analysis of mg, ppm and ppb levels of analyte by appropriate instrumental methods.
Applications: Chemical analysis of hazardous materials, environmental samples, inorganic, organic and biomaterials at trace and ultra trace quantities.
content
Introduction to spectroscopic techniques.
UV - Vis Spectrophotometry, Nephelometry, Turbidimetry, Reflectance Spectrometry, Fluorescence, Phosphorescence Spectrometry.
Flame Emission and Atomic Absorption Spectrometry, Electrothermal AAS, Hydride generation AAS and Flameless mercury analysis.
Inductively Coupled Plasma Atomic Emission Analysis.
Infrared spectrometry.
Introduction to X-Ray techniques, XRF.
Introduction to NMR spectroscopy and mass spectrometry.
Electroanalytical techniques: Potentiometry, Voltametry, Polarography.
Chromatographic analysis: GC, LC, HPLC, Hyphenated techniques.
Errors, statistical methods of data handling.

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  1. Mod-01 Lec-01 Introduction to the Modern Instrumental Methods of Analysis
  2. Mod-01 Lec-02 Atomic Structure
  3. Mod-01 Lec-03 Physical Properties of Electromagnetic Radiation
  4. Mod-01 Lec-04 Interaction of Matter with Radiation
  5. Mod-02 Lec-05 Ultraviolet and Visible Spectrophotometry -1 i. Theoretical Aspects
  6. Mod-02 Lec-06 Ultraviolet and Visible Spectrophotometry -2 ii. Theoretical Aspects
  7. Mod-02 Lec-07 Ultraviolet and Visible Spectrophotometry -3 iii. Theoretical Aspects
  8. Mod-02 Lec-08 Ultraviolet and Visible Spectrophotometry -4 iv. Instrumentation
  9. Mod-02 Lec-09 Ultraviolet and Visible Spectrophotometry -5 v. Instrumentation
  10. Mod-02 Lec-10 Ultraviolet and Visible Spectrophotometry -6 vi. Applications
  11. Mod-02 Lec-11 Fluorescence and Phosphorescence Spectrophotometry 1 i. Theoretical Aspects
  12. Mod-02 Lec-12 Fluorescence and Phosphorescence Spectrophotometry -2 ii. Instrumentation
  13. Mod-02 Lec-13 Fluorescence and Phosphorescence Spectrophotometry -3 iii. Application
  14. Mod-03 Lec-14 Atomic Fluorescence i. Theoretical aspects
  15. Mod-03 Lec-15 X- Ray Analytical Techniques -1 ii. Instrumentation
  16. Mod-03 Lec-16 X- Ray Analytical Techniques -2 iii. Applications
  17. Mod-04 Lec-17 Atomic Absorption Spectrometry -1 i. Theoretical Aspects
  18. Mod-04 Lec-18 Atomic Absorption Spectrometry -2 ii.Theoretical Aspects
  19. Mod-04 Lec-19 Atomic Absorption Spectrometry -3 iii. Instrumentation
  20. Mod-04 Lec-20 Atomic Absorption Spectrometry -4 iv. Instrumentation
  21. Mod-04 Lec-21 Atomic Absorption Spectrometry -5 v. Instrumentation
  22. Mod-04 Lec-22 Atomic Absorption Spectrometry -6 vi. Signal handling
  23. Mod-04 Lec-23 Atomic Absorption Spectrometry -7 vii. Interferences
  24. Mod-04 Lec-24 Atomic Absorption Spectrometry -8 viii. Hydride Generation AAS
  25. Mod-04 Lec-25 Atomic Absorption Spectrometry -9 ix.Cold Vapour Mercury AAS
  26. Mod-04 Lec-26 Electrothermal Atomic Absorption Spectrometry -10 x. Electrothermal Aspects
  27. Mod-04 Lec-27 Electrothermal Atomic Absorption Spectrometry -11 xi. Practical Aspects
  28. Mod-04 Lec-28 Inductively Coupled Plasma Atomic Emission Spectrometry -1 i. Theoretical Aspects
  29. Mod-04 Lec-29 Inductively Coupled Plasma Atomic Emission Spectrometry -2 ii. Instrumentation
  30. Mod-04 Lec-30 Inductively Coupled Plasma Atomic Emission Spectrometry -3 iii.
  31. Mod-05 Lec-31 Infrared Spectroscopy -1 i. Theoretical Aspects
  32. Mod-05 Lec-32 Infrared Spectroscopy -2 ii. Practical Aspects
  33. Mod-05 Lec-33 Infrared Spectroscopy -3 iii. Nondispensive IR, Mass spectrometer
  34. Mod-05 Lec-34 Introduction to Mass Spectrometry
  35. Mod-05 Lec-35 Introduction to Nuclear Magnetic Resonance Spectroscopy
  36. Mod-06 Lec-36 Fundamentals of Electrochemical Techniques -1 i. Introduction
  37. Mod-06 Lec-37 Fundamentals of Electrochemical Techniques -2 ii. Introduction continued
  38. Mod-06 Lec-38 Polarography -1 i. Introduction
  39. Mod-06 Lec-39 Polarography -2 ii. Applications
  40. Mod-07 Lec-40 Chromatography -1 i. Introduction
  41. Mod-07 Lec-41 Gas chromatography -1 i. Instrumentation
  42. Mod-07 Lec-42 Gas chromatography -2 ii. Applications
  43. Mod-07 Lec-43 Gas chromatography -3 iii. Applications