Modern Instrumental Methods of Analysis

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This course is designed to familiarize the students with various instrumental methods of chemical analysis that scientists and engineers come across during their course work and research undertakings.
The participants are introduced to the principles of chemical analysis, matrix effects, detailed instrumentation, operation and interpretation of data, error analysis and statistical methods of data handling.
At the end of the course the student would be able to handle the analysis of mg, ppm and ppb levels of analyte by appropriate instrumental methods.
Applications: Chemical analysis of hazardous materials, environmental samples, inorganic, organic and biomaterials at trace and ultra trace quantities.
content
Introduction to spectroscopic techniques.
UV – Vis Spectrophotometry, Nephelometry, Turbidimetry, Reflectance Spectrometry, Fluorescence, Phosphorescence Spectrometry.
Flame Emission and Atomic Absorption Spectrometry, Electrothermal AAS, Hydride generation AAS and Flameless mercury analysis.
Inductively Coupled Plasma Atomic Emission Analysis.
Infrared spectrometry.
Introduction to X-Ray techniques, XRF.
Introduction to NMR spectroscopy and mass spectrometry.
Electroanalytical techniques: Potentiometry, Voltametry, Polarography.
Chromatographic analysis: GC, LC, HPLC, Hyphenated techniques.
Errors, statistical methods of data handling.

Course Curriculum

Introduction to the Modern Instrumental Methods of Analysis Details 47:46
Atomic Structure Details 55:37
Physical Properties of Electromagnetic Radiation Details 46:47
Interaction of Matter with Radiation Details 55:16
Ultraviolet and Visible Spectrophotometry -1 i. Theoretical Aspects Details 54:14
Ultraviolet and Visible Spectrophotometry -2 ii. Theoretical Aspects Details 54:35
Ultraviolet and Visible Spectrophotometry -3 iii. Theoretical Aspects Details 53:27
Ultraviolet and Visible Spectrophotometry -4 iv. Instrumentation Details 57:41
Ultraviolet and Visible Spectrophotometry -5 v. Instrumentation Details 58:48
Ultraviolet and Visible Spectrophotometry -6 vi. Applications Details 56:38
Fluorescence and Phosphorescence Spectrophotometry 1 i. Theoretical Aspects Details 57:45
Fluorescence and Phosphorescence Spectrophotometry -2 ii. Instrumentation Details 54:7
Fluorescence and Phosphorescence Spectrophotometry -3 iii. Application Details 58:28
Atomic Fluorescence i. Theoretical aspects Details 57:56
X- Ray Analytical Techniques -1 ii. Instrumentation Details 57:35
X- Ray Analytical Techniques -2 iii. Applications Details 58:24
Atomic Absorption Spectrometry -1 i. Theoretical Aspects Details 56:39
Atomic Absorption Spectrometry -2 ii.Theoretical Aspects Details 58:6
Atomic Absorption Spectrometry -3 iii. Instrumentation Details 57:26
Atomic Absorption Spectrometry -4 iv. Instrumentation Details 57:50
Atomic Absorption Spectrometry -5 v. Instrumentation Details 57:51
Atomic Absorption Spectrometry -6 vi. Signal handling Details 57:32
Atomic Absorption Spectrometry -7 vii. Interferences Details 57:33
Atomic Absorption Spectrometry -8 viii. Hydride Generation AAS Details 58:26
Atomic Absorption Spectrometry -9 ix.Cold Vapour Mercury AAS Details 58:39
Electrothermal Atomic Absorption Spectrometry -10 x. Electrothermal Aspects Details 57:7
Electrothermal Atomic Absorption Spectrometry -11 xi. Practical Aspects Details 1:7
Inductively Coupled Plasma Atomic Emission Spectrometry -1 i. Theoretical Aspects Details 57:44
Inductively Coupled Plasma Atomic Emission Spectrometry -2 ii. Instrumentation Details 58:36
Inductively Coupled Plasma Atomic Emission Spectrometry -3 iii. Details 58:42
Infrared Spectroscopy -1 i. Theoretical Aspects Details 58:26
Infrared Spectroscopy -2 ii. Practical Aspects Details 59:17
Infrared Spectroscopy -3 iii. Nondispensive IR, Mass spectrometer Details 57:18
Introduction to Mass Spectrometry Details 57:28
Introduction to Nuclear Magnetic Resonance Spectroscopy Details 56:43
Fundamentals of Electrochemical Techniques -1 i. Introduction Details 58:24
Fundamentals of Electrochemical Techniques -2 ii. Introduction continued Details 58:23
Polarography -1 i. Introduction Details 59:12
Polarography -2 ii. Applications Details 58:53
Chromatography -1 i. Introduction Details 57:18
Gas chromatography -1 i. Instrumentation Details 56:36
Gas chromatography -2 ii. Applications Details 58:40
Gas chromatography -3 iii. Applications Details 58:44

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